1.安徽农业大学茶与食品科技学院 合肥 230036
[ "张海伟,女,1979年3月出生,2008年于中国农业科学院获博士学位,讲师,E-mail:zhanghaiwei@ahau.edu.cn", "ZHANG Haiwei (female) was born in March 1979, and graduated with a doctor degree from Chinese Academy ofAgricultural Sciences in 2008, lecturer, E-mail:zhanghaiwei@ahau.edu.cn" ]
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张海伟, 张雨露, 费晨, 等. 含脂食品辐照标志物2-烷基环丁酮检测技术研究进展[J]. 辐射研究与辐射工艺学报, 2016,34(4):9-16.
Haiwei ZHANG, Yulu ZHANG, Chen FEI, et al. Progress in studies on the detection technique of 2-alkylcyclobutanones in irradiated lipid-containing foods[J]. Journal of Radiation Research and Radiation Processing, 2016,34(4):9-16.
张海伟, 张雨露, 费晨, 等. 含脂食品辐照标志物2-烷基环丁酮检测技术研究进展[J]. 辐射研究与辐射工艺学报, 2016,34(4):9-16. DOI: 10.11889/j.1000-3436.2016.rrj.34.040102.
Haiwei ZHANG, Yulu ZHANG, Chen FEI, et al. Progress in studies on the detection technique of 2-alkylcyclobutanones in irradiated lipid-containing foods[J]. Journal of Radiation Research and Radiation Processing, 2016,34(4):9-16. DOI: 10.11889/j.1000-3436.2016.rrj.34.040102.
对比分析欧盟标准EN1785:2003方法,综述了近年来2-烷基环丁酮(2-Alkylcyclobutanones,2-ACBs)在提取、净化与检测等方面的研究进展。采用乙腈溶剂直接萃取含脂辐照样品中的2-ACBs→商品化固相萃取小柱净化→GC-MS检测是目前替代EN1785的潜力方法。固相微萃取、柱前衍生化及间接酶联免疫等方法具有快速、节约溶剂、低检出限等优点,但需要对操作条件进一步优化。
Recent advances in extraction, purification and detection methods of 2-alkylcyclobutanones (2-ACBs) were reviewed through comparing analysis of the EU standard (EN1785:2003). Using of direct extraction with acetonitrile, purification with commercial solid phase extraction columns and detection with GC-MS for 2-ACBs is probably the potential method which can be alternative of EN1785. The methods of SPME (Solid-phase microextraction), pre-column derivation and indirect ELISA (Indirect enzyme-linked immunosorbent assay) have many advantages including saving analyzing time and organic solvent, and lowering detection limit. However, the relevant operating conditions need to be further optimized.
烷基环丁酮辐照含脂食品检测技术
2-AlkylcyclobutanonesIrradiationLipid-containing foodsDetection technique
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