HPLC SEPARATION OF RADIOLYSIS PRODUCTS OF DEAERATED BAICALIN ETHANOLIC SOLUTION

Cai Zhongli; He Yongke; Wu Jilan

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HPLC SEPARATION OF RADIOLYSIS PRODUCTS OF DEAERATED BAICALIN ETHANOLIC SOLUTION

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- HPLC SEPARATION OF RADIOLYSIS PRODUCTS OF DEAERATED BAICALIN ETHANOLIC SOLUTION
- Journal of Radiation Research and Radiation Processing Vol. 14, Issue 4, Pages: 210-214(1996)
- 作者机构：
  
  1.北京大学技术物理系　北京　100871
  1.厦门火炬开发区光厦楼厦门火炬高技术产业建设发展公司，厦门　361006
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Cai Zhongli, He Yongke, Wu Jilan. HPLC SEPARATION OF RADIOLYSIS PRODUCTS OF DEAERATED BAICALIN ETHANOLIC SOLUTION. [J]. Journal of Radiation Research and Radiation Processing 14(4):210-214(1996)
DOI：

Cai Zhongli, He Yongke, Wu Jilan. HPLC SEPARATION OF RADIOLYSIS PRODUCTS OF DEAERATED BAICALIN ETHANOLIC SOLUTION. [J]. Journal of Radiation Research and Radiation Processing 14(4):210-214(1996) DOI：

摘要

探索反相HPLC分离黄芩甙乙醇溶液辐解产物，特别探讨了酸在淋洗液中的作用，及“液塞”对分离的影响。选用37%CH,3,OH+63%（0.01%CF,3,COOH-H,2,O）为淋洗液，利用梯度流速法，在放大ODS柱上成功地分离了12个无氧黄芩甙乙醇溶液的γ辐解产物。

Abstract

The separation of radiolysis products of deaerated baicalin ethanolic solution by reverse HPLC was studied, especially, the functions of acid in eluents and the influence of solvent strength on separation were discussed. Twelve radiolysis products were successfully separated on the enhanced ODS column with eluent 37%CH,3,OH+63% (0.01%CF,3,COOH-H,2,O).

关键词

黄芩甙高效液相色谱法辐解产物分离

Keywords

BaicalinHPLCRadiolysis productSeparation

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Department Technical Physics, Peking University

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